Identifikasi Senyawa Mdma dan Paracetamol dalam Sampel Urine Menggunakan Metode Kromatografi Lapis Tipis dan Kromatografi Gas – Spektrofotometri Massa (Gc-Ms)

MDMA (3,4-methylenedioximet amphetamine) is a semisynthetic compound derived from stimulant type amphetamine (ATS) which works by triggering the release of serotonin. Paracetamol (acetaminophen) one drug that has an analgesic-antipyretic effect. analysis requires relatively fast method, so TLC method was chosen. The identification test carried out using 3 chromatographic systems, namely methanol: ammonia TA (100:1.5 v/v), butanol TAF (60:40 and Toluene: acetone: ethanol: TAEA (45: 45: 7: 3v/v/v/v). determination system used as standard. results showed sample contained through Hrfc spectrum approaches. Qualitative Analysis Compounds (Acetaminophen) in Urine aims to analyze paracetamol compounds urine qualitatively gas chromatography - mass spectrometry (GC-MS). Extraction samples ethyl acetate, then derivatized BSTFA containing 1% TMCS analyzed – at 1, 2, hours after consuming gave positive for acetaminophen-TMS while 24, 168, 720 consumption they were negative.